dc.contributor.advisor |
Eyduran, Fatih |
|
dc.contributor.author |
Ünsal, Melih |
|
dc.date.accessioned |
2016-01-26T12:34:33Z |
|
dc.date.available |
2016-01-26T12:34:33Z |
|
dc.date.issued |
2013-01-01 |
|
dc.date.submitted |
2013 |
|
dc.identifier.uri |
http://194.27.38.21/web/catalog/info.php?idx=49786821&idt=1 |
|
dc.identifier.uri |
http://hdl.handle.net/11607/1410 |
|
dc.description.abstract |
Bu çalışmada, kenetlenme bileşeni anilinin kullanıldığı primer amino azo boyarmaddesi (p-aminoazobenzen) sentezlenip, bu amino azo boyarmadde ve dietil skuarat arasındaki amitleşme tepkimesiyle de yeni azo grubu içeren esteramid (bileşik 2) sentezlenmiştir. Ayrıca literatürde spektral verileri eksik olan amitleşme tepkimesiyle N-izopropil grubu taşıyan skuaramid (bileşik 1) sentezlenmiştir. Bileşiklerin kimyasal yapıları spektroskopik yöntemler ile (FT-IR, 1H-NMR, 13C-NMR) belirlenmiş ve bileşiklerin görünür bölge absorpsiyon spektrumları üzerine çözücü etkisi incelenmiştir. |
tr_TR |
dc.description.abstract |
In this study, it was obtained that an amino azo dyes (p-aminoazobenzen) synthesized using aniline as the coupling component. The new esteramide (compound 2) including a azo group was synthesized from reaction of the amidation-like between this amino azo dyes and diethyl squarate. Also, an esteramide (compound 1) bearing N- izopropil amino group was synthesized with reaction of the amidation-like which has missing literature. Chemical structures of the compounds were determined using spectroscopic methods (FT-IR, 1H-NMR, 13C- NMR) and the effects of solvent on their absorption spectra were examined. |
tr_TR |
dc.language.iso |
tur |
tr_TR |
dc.publisher |
Adnan Menderes Üniversitesi, Fen Bilimleri Enstitüsü |
tr_TR |
dc.rights |
info:eu-repo/semantics/openAccess |
tr_TR |
dc.subject |
Azo Boyarmadde |
tr_TR |
dc.subject |
Dietil Skuarat |
tr_TR |
dc.subject |
Diazolama |
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dc.subject |
Spektroskopi |
tr_TR |
dc.subject |
Azo Dye |
tr_TR |
dc.subject |
Dietyl Squarate |
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dc.subject |
Diazotization |
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dc.subject |
Spectroscopy |
tr_TR |
dc.title |
Yeni skuaramid maddeleri |
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dc.title.alternative |
New squaramid coumpound |
tr_TR |
dc.type |
masterThesis |
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dc.contributor.department |
Adnan Menderes Üniversitesi, Fen Bilimleri Enstitüsü, Kimya Anabilim Dalı |
tr_TR |